Thermal conductivity is generally the tool of choice for quantification of fixed gases, particularly lighter-than-air gases. Unfortunately, gas chromatography-thermal conductivity detectors (GC-TCDs) are difficult to introduce in first- and second-year chemistry courses where the cost and number of instruments, as well as the space required, is…

The purpose of this communication is to describe and document the challenges of delivering a general chemistry laboratory experience to students and of moving toward multiple small assessments and away from high-stakes examinations. By leveraging of activities that were already in place prior to the pivot to online learning, namely, an electronic…

Lab courses are a significant component of biochemistry and molecular biology (BMB) education. In teaching the labs, we combine established techniques with novel approaches. Lab formats have also moved from traditional cookbook style labs to guided inquiry to course-based undergraduate research experiences (CUREs), where faculty bring their own…

Biodiesel is an important biomass, largely employed in the transport sector and produced from vegetable oils. Additionally, waste cooking oils may be reused to produce biodiesel fuel, minimizing environmental pollution. A laboratory experiment that affords a widespread way to discuss degradation concepts and tools for used vegetable oil…

For conducting laboratory experiments on Fresnel diffraction, the use of a simple point light source from an LED and the application of a modern smartphone for photographing the diffraction patterns are proposed. The developed devices allow the experiments to be carried out under normal laboratory lighting.

When injecting dye into a vortex, one finds that the dye remains captured around the vortex core over minutes, despite the fact that the vortex (and the dyed region) is strongly time-dependent. According to a recent theory, three-dimensional time-dependent vortices should be defined as rotating, material-holding regions of the fluid. Vortices…

A modular and target-group oriented online video library with 48 videos was developed and produced in order to reduce the complexity of an introductory organic chemistry laboratory class. The library comprises three different types of videos: "Tutorials" explaining fundamental laboratory techniques, "Do nots" pointing students…

A continuous flow photopinacol coupling of benzophenone has been developed and implemented in the undergraduate laboratory. This photoreduction was accomplished using 2-propanol as an H atom donor and cosolvent in the reaction. The simple and inexpensive UV light source and flow reactor design (less than $350/photochemical flow system) provide an…

Lock-in amplifiers (LIAs) are commonly used in chemistry laboratories to improve noise-to-signal ratios. Constructing and testing a suitably designed LIA provide undergraduate students with an excellent opportunity to learn about theory, construction, and applications of LIA. In particular, students can learn about time-dependent behavior and…

An undergraduate organic chemistry experiment has been developed that features asymmetric synthesis of an enantioenriched secondary alcohol, followed by determination of its absolute configuration using the competing enantioselective conversion (CEC) method. Students are given a ketone and an unknown enantiomer of CBS (Corey-Bakshi-Shibata)…

Physics experiments powered by a universal serial bus (USB) connection are becoming increasingly common. With teachers going through so many batteries each year, USB-powered physics provides an economical and environmentally friendly alternative. In this article, the authors discuss several ways that USB power can provide a convenient way to do…

This paper describes the development, final design and validation of an instrument that measures a range of student interactions and satisfaction in undergraduate chemistry laboratories. Student surveys or conceptual and attitudinal instruments are widely used techniques for collecting relevant information on student learning. However, there is a…

Enzymes are widely applied in different industries, like pharmaceutical, food, biofuel, and waste valorization. However, the enzyme operating conditions are very limited. So, in most industrial processes, enzymes are not efficient, due to the use of harsh conditions, like organic solvents, extreme pH, and temperature. Immobilization arises as a…

Few laboratory exercises exist that introduce undergraduate students to both the concepts and instrumentation used in rotational spectroscopy. Because of this gap in undergraduate laboratory training, a teaching laboratory for the pure rotational spectroscopy of benzonitrile has been developed and reported. Owing to benzonitrile's recent discovery…

A working knowledge of Artificial Neural Networks is rapidly becoming critical for navigating the modern world. Although the last few years have seen an explosion of the use of these tools in research, and there are many do-it-yourself articles on the web, they have not yet filtered down to wide implementation in introductory courses. I report…