Reports on the status of nuclear magnetic resonance (NMR) from theoretical and clinical perspectives, reviewing NMR theory and relaxation parameters relevant to NMR imaging. Also reviews literature related to modern imaging strategies, signal-to-noise ratio, contrast agents, in vivo spectroscopy, spectroscopic imaging, clinical applications, and…

Proposes use of two experiments to sample and analyze contaminents in the laboratory. Experiments focus on estimating hydrogen sulfide levels in the general chemistry laboratory during qualitative analysis and determining the concentration of organic vapors associated with organic chemistry laboratories. (JN)

Provided are experiments to acquaint students with basic spectrophotometer components and their functions, to use the instrument in an openended-experiment, and to use Beer's Law in several different ways. In addition, the detectability (tolerance) of the spectrophotometer with visual detection limits is provided as an optional activity. (JN)

Background information, procedures, and results are provided for an experiment in which lead-210 is separated from bismuth-210 and polonium-210 by means of solvent extraction of their diethyldithiocarbamate complexes. The method involves a simple extraction procedure which allows complete separation of lead-210 from commercially available…

Although determination of phosphorus is important in biology, physiology, and environmental science, traditional gravimetric and colorimetric methods are cumbersome and lack the requisite sensitivity. Therefore, a derivative activation analysis method is suggested. Background information, procedures, and results are provided. (JN)

Discusses working implementations of artificial intelligence systems for chemical laboratory applications. They include expert systems for liquid chromatography, spectral analysis, instrument control of a totally computerized triple-quadrupole mass spectrometer, and the determination of the mineral constituents of a rock sample given the powder…

Literature on analytical methods related to the functional groups of 17 chemical compounds is reviewed. These compounds include acids, acid azides, alcohols, aldehydes, ketones, amino acids, aromatic hydrocarbons, carbodiimides, carbohydrates, ethers, nitro compounds, nitrosamines, organometallic compounds, peroxides, phenols, silicon compounds,…

Presents a literature review on methods used to analyze organic elements. Topic areas include methods for: (1) analyzing carbon, hydrogen, and nitrogen; (2) analyzing oxygen, sulfur, and halogens; (3) analyzing other elements; (4) simultaneously determining several elements; and (5) determing trace elements. (JN)

Reviews literature covering developments of column liquid chromatography during 1982-83. Areas considered include: books and reviews; general theory; columns; instrumentation; detectors; automation and data handling; multidimensional chromatographic and column switching techniques; liquid-solid chromatography; normal bonded-phase, reversed-phase,…

Background information, procedures, and results are provided for an experiment in which students: (1) construct an immobilized penicillinase electrode; (2) evaluate electron response as a function of penicillin concentration; and (3) study effects of solvent compositions, ionic strength, and equilibrium time upon electrode response. (JN)

Background, procedures, and results are provided for an experiment which examines, through electron spin resonance spectroscopy, complex species formed by cupric and 2,6-dihydroxybenzoate ions in aqueous solutions. The experiment is illustrative of several aspects of inorganic and coordination chemistry, including the identification of species…

Outlines an approach for helping student teams assign roles to each participant for doing portions of the experiment and writing the report. Discusses teaching of technical report writing as outlined in the Style Manual of the American Institute of Physics. (MLH)

Provides a listing of all state guidelines and regulations pertaining to use of hypodermic syringes, eye safety, and animal care in biology and general science laboratories. (SL)

Describes an advanced undergraduate materials science course in which each student conducts two independent laboratory projects and is required to submit a formal lab report at the end of each project. (MLH)

Explains a scientific approach to accident prevention and outlines the safety aspects associated with the handling of chemicals in the secondary school. Provides a check list of unsafe acts and conditions, outlines features of good laboratory management, and gives hints for combating the effects of inflation on science budgets. (GS)