Explores the relationship between scientists' orientation to one another and to an experimental apparatus, analyzing as data a videotaped authentic interaction among co-workers in a chemistry laboratory. Demonstrates how the scientists display systematic orientation to the apparatus as their common spatial point of reference and the physical…

Provides descriptions of a range of resources and methods that can be used to produce metals such as titanium, vanadium, chromium, manganese, iron, and molybdenum. Details on equipment and safety precautions are also outlined. (DDR)

Describes a technique for using lecture-laboratory facilities and faculty office facilities to provide students a site for intensive laboratory exercises. Provides a layout of the lecture-laboratory facilities and energy systems of the facilities. Presents an instructional example on the concept of the natural frequency of single-degree-of-freedom…

Detailed is a method in which short pieces of teflon tubing may be used for collection tubes for collecting preparative fractions from gas chromatographs. Material preparation, laboratory procedures, and results of this method are discussed. (CW)

Described is a procedure for studying the trajectories of projectiles using ball bearings and aluminum foil. Trajectories were measured with and without the effects of air resistance. Multiflash photography was used to determine the flight paths of all objects. (KR)

Using Fourier transformation methods in nuclear resonance has made possible increased sensitivity in chemical analysis. This article describes data acquisition, data processing, and the frequency spectrum as they relate to this technique. (CW)

Nuclear magnetic resonance and infrared are two spectroscopic methods that commonly use the Fourier transform technique. Discussed are the similarities and differences in the use of the Fourier transform in these two spectroscopic techniques. (CW)

Discussed are the mechanisms of nuclear magnetic relaxation, and applications of relaxation times. The measurement of spin-lattice relaxations is reviewed. It is stressed that sophisticated techniques such as these are becoming more important to the working chemist. (CW)

Presented is an experiment to show the connection between spectroscopy and thermochemistry by examining the spectra of atomic sodium and diatomic sodium. Background information; a description of the apparatus; procedures; calculations; and energy diagrams are included. (CW)

Described is a microscale chemistry laboratory in which students perform a kinetics experiment, plot the data, and get consistent results for the "k" value. Different aspects of this type of reaction are demonstrated. Experimental apparatus and procedures are detailed. (CW)

Described is a microscale organic chemistry laboratory which involves the separation and purification of a mixture consisting of a strong organic acid, a weak organic acid, an organic base, and two neutral compounds. Reinforced are the basic principles of acid/base chemistry and the physical properties of the associated functional groups. (CW)

Described is a microscale chemistry laboratory in which a dipeptide is synthesized from its component amino acids and analyzed using chiral-phase thin-layer chromatography. Experimental procedures, and materials are discussed. Twelve references are listed. (CW)

Described is a demonstration in which the reaction sequence can be easily followed since the reactant, intermediates, and the final product have intense and different colors. Materials and procedures for this demonstration are discussed. (CW)

Three uses of this method with sandstone, desert varnish, and granite weathering are described. Background information on this technique is provided. Advantages of this type of microscopy are stressed. (CW)

Presents data for instructors on the current state of ultraviolet-visible detector technology and gives sources of further information. Described are the mechanisms and characteristics of photomultiplier tubes and array detectors. Lists 15 references. (YP)