In this article, we discuss the replication of a forgotten chemical instrument in the context of undergraduate chemistry education. Together with students, we have attempted to replicate an eighteenth century "eudiometrical" procedure. Eudiometry was the practice of measuring the "goodness" of the air by looking at the volume…

To deliver state-of-the-art battery knowledge to undergraduates, we designed a feasible experiment to prepare flexible packaging batteries, aiming to reproduce industrial flexible packaging batteries in general chemistry laboratories. In our procedure, the materials involved are inexpensive, safe, and easy to use. No organic solvents or toxic…

Titration is an important experimental skill that every chemistry educator and learner must master. Titration is often the method of choice in the science laboratory courses in secondary and postsecondary schools. During acid-base titration, chemistry learners are always told about salt formation. However, a practical visualization of the salt…

This paper outlines a comprehensive teaching laboratory course program that centers on titration analysis, a timeless and essential technique in analytical chemistry spanning various disciplines, such as environmental science, medicine, and industry. In these fields, titration analysis is paramount for determining the concentrations of substances…

Metabolic Control Analysis (MCA) is a systems biology approach that measures the control of a metabolic step on the overall flux of a metabolic pathway. In undergraduate courses in biochemistry, learning of MCA can be encouraged by experimental activities demonstrating practical applications of the MCA theory. In this work, we present a laboratory…

By hosting a college students' laboratory skills contest, we provide an interesting activity for students to cultivate good laboratory practices and thereby improve their laboratory skills. The substance of this contest is the detection of the hardness of water, which involves numerous laboratory skills such as solution preparation, weight by…

Chemists have always designed and deployed cross-disciplinary approaches that interface chemistry with other disciplines to proffer solutions to many human problems. We designed a laboratory experiment that implements chemistry concepts in a biological model to prime undergraduate students to appreciate interdisciplinarity as an approach to…

Exposure to real-life applications of quantitative analysis techniques based on two gas chromatography (GC) experiments was provided to a large cohort of sophomore-level students. In one experiment, students assessed blood alcohol content by internal standardization using a homemade headspace system similar to methods implemented in forensic…

Amides are usually prepared using amines and acyl halides, which often implies a two-step procedure. Alternatively, coupling reagents can be used in a single-step reaction with good yields, which seems to be suitable for organic chemistry laboratory classes. This work was designed to synthesize "N"-hexylcinnamamide through a one-step…

We report a research-enhanced undergraduate laboratory practical in which students synthesize and characterize color-controllable, stable silver nanoparticles for use in a simple catalytic reaction analyzed by UV-vis spectroscopy. The practical has been prepared for students using electronic laboratory notebooks, enables collaborative data…

A new two-step experiment has been designed and developed for the curriculum of the Organic Chemistry Laboratory 2 (CHEM2240L) sophomore course at Xavier University of Louisiana, in New Orleans. Initially, cyclohexanol was converted to cyclohexanone using bleach as the oxidizing agent followed by the formation of the cyclohexanone oxime. However,…

[superscript 1]H NMR spectroscopy is a molecular characterization technique that is ubiquitously used in research and teaching laboratories alike. Strategic deuteration of molecules is a commonly employed technique in the deconvolution of [superscript 1]H NMR signals. Here this approach is applied in a second-year chemistry course in which…

An integrated and research-focused laboratory experiment is developed to introduce the "antenna effect" occurring in luminescent lanthanide complexes to students. Students synthesized a lanthanide metal-organic framework (Ln-MOF) with the formula of [Eu(BTPCA)(H O)]·2DMF·nH[Subscript 2]O (Eu-BTPCA, H[subscript 3]BTPCA =…

An experiment for the undergraduate organic chemistry laboratory involving a method for the isolation of eugenol from cloves has been developed. The experiment employs microwave-assisted extraction (MAE) of the essential oil from whole cloves using aqueous ethanol and the subsequent isolation of eugenol by acid-base extraction. The MAE allows for…

This laboratory experiment, designed for undergraduate nonmajors or advanced high school students, attempts to demystify the technique of spectrophotometry by utilizing a hands-on, real-world approach. Modification of the reaction for the formation of Fe[(bpy)[subscript 3]][subscript 2+] allows students to interact with vitamin C, a compound with…