As a fundamental part of their chemical education, first-year undergraduate students are substantially involved in laboratory activities. Despite the specific teaching staff choices on the main laboratory aims, students normally receive a vast amount of information during these activities. Apart from understanding theoretical content, fundamental…

Practical skills in science education, defined as those developed through the observation, demonstration, manipulation, and application of scientific principles, valued in both academia and industry, feature conspicuously in curriculums the world over. Efficiently imparting such skills to students necessitates access to scientific equipment of…

Comfort whilst camping overnight during outdoor pursuits is based on pain free and warm sleeping arrangements and is highly dependent on the performance of the sleeping bag and sleeping mat. In adventurous and challenging situations, performance can contribute to safety and expedition success. From the manufacturer's point of view, thermal…

Could Usain Bolt achieve what teachers often fail to do? Could this famous Olympic winner challenge and motivate students to study mechanics and introduce them to the principles of physics in a fun way, outside of the classroom? In order to answer these questions, we "invited" for one semester the world record holder to visit our Greek…

The classroom jumping ring demonstration is nearly always performed using alternating current (AC), in which the ring jumps or flies off the extended iron core when the switch is closed. The ring jumps higher when cooled with liquid nitrogen (LN2). We have performed experiments using DC to power the solenoid and find similarities and significant…

Variable temperature NMR spectroscopy is used to determine the ?H° and ?S° of hydrogen bond formation in a simple diamide. In this two- or three-day experiment, students synthesize N,N'-dimethylmalonamide, dimethylsuccinamide, dimethylglutaramide, or dimethyladipamide from methylamine and the corresponding diester (typically in 50% recrystallized…

An integrative laboratory study addressing fundamentals of enzyme catalysis and their application to reactors operation and modeling is presented. Invertase, a ß-fructofuranosidase that catalyses the hydrolysis of sucrose, is used as the model enzyme at optimal conditions (pH 4.5 and 45 °C). The experimental work involves 3 h of laboratory time…

An asymmetric synthetic experiment that encompasses both diastereoselectivity and enantioselectivity is described. In this experiment, Zn-mediated allylation of an ("R")-"N"-"tert"-butanesulfinyl imine is first performed to obtain either diastereomer using two different solvent systems, followed by oxidation of the…

Measuring the heat capacity ratios, [gamma], of gases either through adiabatic expansion or sound velocity is a well established physical chemistry experiment. The most accurate experiments depend on an exact determination of sound origin, which necessitates the use of lasers or a wave generator, where time zero is based on an electrical trigger.…

Two experimental techniques of solid-liquid extraction are compared relating to the lab-scale production of lemon liqueur, most commonly named "limoncello"; the first is the official method of maceration for the solid-liquid extraction of analytes and is widely used to extract active ingredients from a great variety of natural products;…

The formation and the hydrolysis of organic salts produced by the titration of a 0.1 M solution of the following amines: methyl-, dimethyl-, trimethyl-, ethyl-, diethyl-, and triethylamine with a 0.1 M solution of acetic, chloroacetic, and dichloracetic acids are studied. The pK[subscript b] of the amine and the pH at the end point were determined…

Since physics is often a service course for college students, it is important to incorporate everyday examples in the curriculum that inspire students of diverse backgrounds and interests. In this regard, baseball has been a workhorse for the physics classroom for a long time, taking the form of demonstrations and example problems. In this…

Digital storytelling is a technology application that has emerged as a powerful teaching and learning tool that engages both teachers and students. Digital storytelling allows students to become creative storytellers through selecting a topic, conducting research, writing a script, and developing the story. However, the use of digital storytelling…

Engaging undergraduates in the environmental consequences of fossil fuel usage primes them to consider their own anthropogenic impact, and the benefits and trade-offs of converting to renewable fuel strategies. This laboratory activity explores the potential contaminants (both inorganic and organic) present in the raw fuel and solid waste…

Samples of a composite hydrogel incorporating clay (Laponite XLG and S-482) nanoparticles were prepared using N-isopropylacrylamide. The hydrogels were formed via a radical-initiated addition polymerization using potassium persulfate and N,N,N',N'-tetramethylethylenediamine. Students then measured the force required to stretch the gels and…