Explains a laboratory exercise where 2-methylpyrazinepentacyanoiron (II) is synthesized by thermal and photochemical pathways. (GA)

Describes a simple undergraduate experiment in chemistry dealing with the "solvent effects" in nuclear magnetic resonance (NMR) spectroscopy. Stresses the importance of having students learn NMR spectroscopy as a tool in analytical chemistry. (TW)

Describes an experiment in which students become familiar with the organic chemistry extraction process, perform analyses by thin layer and column chromatography, and use the absorption spectrum (obtained from a spectrophotometer) for identification. List of materials needed and procedures used are provided. (JN)

Describes an experiment enabling students to apply concept of diffraction, determine limits of their color perception, learn how to measure wavelength with a simple apparatus, observe continuous and line spectra, and associate colors with corresponding wavelengths. The homemade diffraction-grating spectrometer used is easily constructed. (JN)

Electronic energy levels in noble gas atoms may be determined with a simple teaching apparatus incorporating a resonance potentials tube in which the electron beam intensity is held constant. The resulting spectra are little inferior to those obtained by more elaborate electron-impact methods and complement optical emission spectra. (Author/SK)

Describes an advanced undergraduate laboratory experiment designed to give the senior chemistry student an opportunity to apply several synthetic and purification techniques as well as possibilities for the application of NMR spectroscopy. (CS)

Presents methods by which undergraduate students gain practice in ESR spectroscopy. (CS)

This experiment demonstrates the polarization properties of the transition moment, vibronic activity in an excited state, cyrogenic techniques, crystal site splitting, and the use of mixed crystals. (BB)

Presents a discussion for the principles of a Fourier Transform infrared spectrophotometer which is intended to provide chemists with a basic understanding of these principles. (HM)

Any overhead projector easily can be converted into a simple spectrometer by placing a piece of diffraction grating over the projecting lens. A detailed description of the apparatus and suggested spectroscopy experiments are included. Demonstrations can utilize solutions of cobalt chloride, potassium permanganate, potassium dichromate, or…

Describes an experiment for advanced-level undergraduate students for extending student experiences involving recording and interpreting infrared (IR) and nuclear magnetic resonance (NMR) spectra from reactions of organometallic compounds. Experimental procedures, analyses and structural assignments, and suggestions for extension and modification…

Studies the polarization effect on water by cations and anions. Describes an experiment to illustrate the polarization effect of sodium, lithium, calcium, and strontium ions on the water molecule in the hydration spheres of the ions. Analysis is performed by proton NMR. (MVL)

Develops a lab experiment for introductory instrumental analysis that requires interference studies and optimizing of conditions. Notes the analysis of the aspirin is by visible spectrophotometric assay. Gives experimental details and discussion. (MVL)

Describes absorption spectroscopy experiments that allow students to explore the mechanisms by which sunscreens and sunglasses provide protection from ultraviolet radiation. Exposes students to absorption phenomena in an engaging way. (DDR)

The use of complex instruments for chemical analysis is becoming increasingly important. Unfortunately, because of school budgetary constraints, many students are not exposed to these methods until they reach the college level. When students do have access to sophisticated instruments, they often view them as black boxes, with little or no…