In this article we describe the construction of a low-cost electronic device to adapt the widespread traditional approach of Analytical Chemistry teaching into laboratory experimentation based on the guided research model. To this aim we construct a portable electronic instrument based on the Arduino microcontroller and use it to develop various…

In general, undergraduate experimental physics laboratories do not usually have experiments designed to address rolling friction and to measure the value of the rolling friction coefficient. This work explores an experiment, which has the potential to arouse students' curiosity about rolling friction by addressing a counterintuitive aspect of the…

Nuclear magnetic resonance (NMR) spectroscopy has become a cornerstone tool for studying a variety of molecular features in advanced chemistry laboratories. In this experiment, students prepare a pyrrole-[beta]-amide via a one-pot, three-step synthesis and use NMR spectroscopy to confirm its molecular structure. In addition, variable temperature…

Green chemistry metrics and life-cycle analysis (LCA) were used to assess inefficiencies in two current organic chemistry experiments conducted in third-year organic chemistry to synthesize ("E")-stilbene from benzaldehyde. An alternative Wittig-based, greener, one-pot experiment using the same starting material was selected as a vehicle…

A research-style laboratory experiment for advanced undergraduate students is described, which includes the synthesis, characterization, and properties (porosity, stability, amphipathy) testing of the composite [Cu[subscript 2](BTC)[subscript 4/3](H[subscript 2]O)[subscript 2][subscript 6][HPW[subscript 12]O[subscript 40]·(C[subscript…

This work reports the first use of rubber latex waste as the hydrophobic reagent for a low-cost, simple, and rapid fabrication of a paper towel-based experimental device (PTED) with a circular design of 5 mm to demonstrate the factors affecting chemical equilibrium; this serves as a user-friendly means for a laboratory experiment. The illustration…

Introducing chemical equilibrium concepts in undergraduate general chemistry promotes improved understanding of chemical reactions. We have developed an engaging laboratory experiment exploring the equilibrium of cobalt complexation in alcohols using UV-vis spectroscopy and successfully implemented in a large general chemistry class of 378…

A contemporary undergraduate laboratory experiment incorporating parallel microscale experimentation was developed for the well-defined palladium catalyzed Suzuki-Miyaura cross coupling of 4-fluorophenylboronic acid with both 4-chloro- and 4-bromoanisole using 11 diverse phosphine ligands and one ligandless control. This laboratory introduces…

If a smooth ball is dropped vertically without spin on a smooth horizontal surface then one might expect the ball to bounce vertically without spin. If it does not then the centre of mass of the ball does not coincide with its geometric centre. An experiment is described where a billiard ball and a superball are deliberately biassed by adding a…

Chemical energy storage and use is a critical part of a sustainable world. In this laboratory experiment, students construct and use an inexpensive hydrogen fuel cell to power a calculator or a clock. The reusable cells are prepared from plastic syringes and a nickel mesh that is coated with a palladium metal catalyst by electroless deposition.…

The stately fall of magnets through conducting pipes is a favorite classroom and laboratory activity used in teaching electromagnetic induction, Lenz's law, eddy currents, electromagnetic braking, and even Newton's third law. When a neodymium magnet is used, the terminal velocity is reached in just a few milliseconds as the induced eddy currents…

A standard problem for physics students is to calculate or measure the acceleration of an object down an inclined plane. Additional information can be obtained by measuring the angular acceleration as well as the linear acceleration. An experiment is described where a billiard ball was filmed as it rolled down an inclined plane at different…

To deliver state-of-the-art battery knowledge to undergraduates, we designed a feasible experiment to prepare flexible packaging batteries, aiming to reproduce industrial flexible packaging batteries in general chemistry laboratories. In our procedure, the materials involved are inexpensive, safe, and easy to use. No organic solvents or toxic…

A single latent fingerprint consists of ~50 µg of matter for which the anionic content often provides a differentiating characteristic between individuals. This forensic-themed, analytical chemistry experiment exploits this difference and has students employ ion-exchange chromatography to quantitatively analyze the anionic content of both…

The abstract definition of electric power as "ability of a voltage source to do work" or quantitatively as "energy per unit charge" is preceded by a qualitative description in terms of the existence of surface charges. These surface charges and the associated electric fields can be demonstrated experimentally and allow a causal…