The Hofmeister series is a recurring trend that ranks ions' abilities to influence various aqueous processes in solution. Herein, a set of project-based experiments was developed for students in an upper-level physical chemistry laboratory to investigate the specific ion effects on the thermodynamics of caffeine partitioning between aqueous and…

The ability to visualize chemical processes can be an asset in a teaching laboratory. Despite the advances in laboratory technology, apparatuses used in the teaching of simple thermodynamics concepts, such as exothermic/endothermic reactions, historically remain unchanged and can benefit from a fresh perspective. The recent incorporation of…

We report the findings of an empirical study that investigated whether the source of data--firsthand or secondhand data gained from lab work experiments--has an influence on students' learning outcomes. Results indicate that students' choice of a correct or incorrect hypothesis for a pendulum lab experiment on the influence of the mass of the bob…

A straightforward protocol for the preparation of the colorful and air-stable diphenyl ditelluride is described. In one laboratory session, students isolate their product and characterize it via melting point determination, mass spectrometry, and NMR spectroscopy ([superscript 1]H, [superscript 13]C­{[superscript 1]H}, and [superscript…

Hydrogen production from electrochemical water splitting via hydrogen evolution reaction (HER) powered by sustainable energy has been recognized as one of the most promising alternatives to traditional fossil fuels. To integrate the fundamental knowledge of chemistry, electrochemistry, and materials science with practical application and…

We developed a single crystal X-ray crystallography experiment based on the crystal structure of sucrose (table sugar), and a more challenging experiment using Epsom salt. Both crystals are readily available in X-ray quality crystalline form. In these experiments, students mounted a crystal on a MiTeGen loop and analyzed it using a Rigaku XtaLAB…

The design and operation of an inverted cone, scalable vapor condenser, drawing cooling air from beyond the boundary layer and optionally working as a part of a gastight setup, are described and discussed. Besides its main use as a reflux condenser, it can also be used in one-plate distillations.

In this supplement to our second-year supercapacitor lab (Bringing Real-World Energy-Storage Research into a Second-Year Physical-Chemistry Lab Using a MnO[subscript 2]-Based Supercapacitor. "J. Chem. Educ." 2018, 95 (11), 2028-2033), we incorporate a color indicator as indirect evidence for the manganese oxide's pseudocapacitive…

A six-laboratory session biofilm-focused biochemistry laboratory module is described. Through just six four-hour laboratory sessions over three weeks, students first master background knowledge and fundamental experimental techniques to explore questions involving bacterial biofilms at the interface of microbiology and biochemistry and then…

The study of gels and their properties is a compelling topic both technologically and scientifically, and should therefore be emphasized in chemistry and material science syllabuses. In the present laboratory experiment, we propose two experiences, aimed at introducing gelation and gel transport properties using silica gels made from sodium…

A laboratory exercise on the interaction between the herbicide pendimethalin (PM) and goat serum albumin (GSA), a carrier protein present in mammalian blood circulation, is described. Fluorescence spectroscopy was used to study the binding reaction between PM and GSA. Titration of a constant amount of the protein (GSA) with increasing ligand (PM)…

Next generation sequencing has revolutionized molecular biology and has provided a mechanism for rapid DNA and RNA sequence analysis. Yet, there are few resources to introduce next generation sequencing into the undergraduate biochemistry and molecular biology curriculum. Herein, we describe the design, execution, and assessment of a four-week…

Demonstration of a colorimetric approach for nucleic acid detection represents an attractive educational experiment for chemistry undergraduate students in the time of coronavirus pandemic. Herein, a rapid and vivid detection method that visualizes the presence of a specific DNA sequence is described. The plasmon resonance of gold nanoparticles…

A two-week summer camp was designed, implemented, and then updated for high school students focusing on organic chemistry, solar energy, and green chemistry principles. Students learn about laboratory safety, perform organic reactions, go on field trips, and take part in interactive lessons that focus on both fundamental chemistry topics as well…

In this article, we present a low-cost lab experience, enhanced by new technologies and easy to execute. The objective of the experiment is to explore the moment of inertia of a fidget spinner quantitatively. Our choice was to integrate the teaching of physics with the use of a popular toy, the fidget spinner, very popular among young people and…