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Kjonaas, Richard A.; Tucker, Ryand J. F. – Journal of Chemical Education, 2008
The use of permanent magnet [to the thirteenth power]C NMR in large-section first-semester organic chemistry lab courses is limited by the availability of experiments that not only hinge on first-semester lecture topics, but which also produce at least 0.5 mL of neat liquid sample. This article reports a discovery-based experiment that meets both…
Descriptors: Organic Chemistry, College Science, Laboratory Experiments, Introductory Courses
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Brigandi, Laura M.; Leber, Phyllis A.; Yoder, Claude H. – Journal of Chemical Education, 2005
A project involving the synthesis of several naturally occurring copper double salts using simple aqueous conditions is reported. The ions present in the compound are analyzed using colorimetric, gravimetric, and gas-analysis techniques appropriate for the first-year laboratory and from the percent composition, the empirical formula of each…
Descriptors: Chemistry, Science Instruction, Undergraduate Students, Introductory Courses