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Direct linkCooke, Jason; Hebert, Dominique; Kelly, Joel A. – Journal of Chemical Education, 2015
This work describes a convenient and reliable laboratory experiment in nanochemistry that is flexible and adaptable to a wide range of educational settings. The rapid preparation of yellow colloidal silver nanoparticles is achieved by glucose reduction of silver nitrate in the presence of starch and sodium citrate in gently boiling water, using…
Descriptors: Science Instruction, Science Laboratories, Science Experiments, Laboratory Experiments
Cooke, Jason; Lightbody, Owen C. – Journal of Chemical Education, 2011
Experiments are described for the preparation of imidazolium chloride precursors to "N"-heterocyclic carbenes and their cyclopentadienyl nickel chloride derivatives. The syntheses have been optimized for second- and third-year undergraduate laboratories that have a maximum programmed length of three hours per week. The experiments are flexible and…
Descriptors: Chemistry, Laboratory Experiments, Science Experiments, Undergraduate Students
Cooke, Jason; Berry, David E.; Fawkes, Kelli L. – Journal of Chemical Education, 2007
The photochemical synthesis and subsequent ligand exchange reactions of Ru(CO)[subscript 4] (eta[superscript2]-alkene) compounds has provided a novel experiment for upper-level inorganic chemistry laboratory courses. The experiment is designed to provide a system in which the changing electronic properties of the alkene ligands could be easily…
Descriptors: Inorganic Chemistry, Science Education, Laboratory Experiments, Science Experiments
