A major obstacle that teachers face when they begin their spectroscopy lessons is the lack of a spectrophotometer, mostly due to its relatively high cost. In the present study, the construction of a low-cost do-it-yourself type of instrument is reported. Its construction, as a part of a problem-based scenario, would also help students to enhance…

Nuclear magnetic resonance (NMR) spectroscopy is commonly introduced to students in the classroom, but its hands-on use in undergraduate laboratories is far less common. The significant costs to purchase and maintain a traditional high-field NMR spectrometer means that many institutions cannot offer this service to their students. Benchtop NMR…

Ultraviolet (UV)-visible (Vis) spectroscopy is widely used in all modern laboratories as a routine method of analysis. The monitoring of chemical reactions in an aqueous solution involving a gas product is a demanding task but particularly for oscillatory reactions which are obtainable in a narrow concentration range. In this work, the…

Techniques and instrumentation that involve fluorescence are used in many careers related to biology and biochemistry. However, due to the expense of instrumentation, the theory and practice of fluorescence spectroscopy is commonly concentrated in instrumental analysis in most curricula, a class rarely required for biology and biochemistry majors.…

A low-cost multispectral imager was built using a multiwavelength LED PCB (light-emitting diode printed circuit board), 3D printed housing, and a monochrome camera, and it was controlled via National Instruments LabVIEW software coupled with some simple electronics. Multivariate data analysis was performed using freely available software packages.…

Few laboratory exercises exist that introduce undergraduate students to both the concepts and instrumentation used in rotational spectroscopy. Because of this gap in undergraduate laboratory training, a teaching laboratory for the pure rotational spectroscopy of benzonitrile has been developed and reported. Owing to benzonitrile's recent discovery…

A dual-function student-crafted instrument is described as part of a laboratory activity aimed to teach both the principles and practical aspects of absorption spectroscopy to secondary and introductory undergraduate students. Using minimal changes in an arrangement that is based on interlocking bricks and low-cost components, both a fluorometer…

The importance of utilizing spectroscopic techniques for unraveling structural and compositional changes in nonreacting and reacting systems is unquestionable. Nowadays, efforts are directed towards the introduction of relevant spectroscopic techniques to undergraduate students in order to prepare them for future careers in industry and academia,…

Process analytical technologies (PATs) are used in the pharmaceutical and other industries to monitor chemical processes in real-time with analytical instrumentation. Each PAT analyzer brings its own advantages and disadvantages to the process, and multiplexing PAT analyzers can be advantageous as they can provide confirmatory measurements and…

Chromatography is a ubiquitous technique in analytical chemistry, and high-performance liquid chromatography (HPLC) is the industry standard for quantitation of components in solution mixtures. However, demonstrating the principles of liquid chromatography to undergraduates via HPLC-based experiments often proves ineffective because of the fully…

Student-built photometers are recognized as being useful tools in teaching laboratories that help students understand the concepts behind experimental measurements, and several devices have been reported that employ photoresistors as the detector of choice. We demonstrate here an improvement over these instruments and the analyses thereof,…

Mass spectrometers are ever-increasingly powerful, user-friendly, and affordable. Thus, the addition of mass spectrometry experiments into the undergraduate laboratory curriculum is now both feasible and an effective tool to introduce students to relevant instrumentation. Here an experiment demonstrating the use of a high-resolution electrospray…

A simple computer interface for controlling a compact spectrograph for use as a spectrophotometer in an undergraduate teaching laboratory was developed. The project was implemented on a Raspberry Pi computer which permits the integration of a light source into the software. The interface was written in Python to facilitate modification by the user…

Smartphones, coupled with small mobile sensors, make it possible to work with near-infrared (NIR) spectroscopy in science classrooms. NIR spectroscopy has become a standard analytical technology in various industries. These new devices enable students to create their own data in real time. This article presents an inquiry-based teaching unit, in…

One challenge of teaching chemical analysis is the proliferation of sophisticated, but often impenetrable, instrumentation in the modern laboratory. Complex instruments, and the software that runs them, distance students from the physical and chemical processes that generate the analytical signal. A solution to this challenge is the introduction…