In an effort to further develop critical thinking and problem solving skills, a guided-inquiry-based, multioutcome organic chemistry synthesis and characterization experiment was developed. Students were provided with the protocol for a time-saving microwave-assisted acetanilide synthesis reaction from acetic anhydride and an unknown primary aryl…

Amides are usually prepared using amines and acyl halides, which often implies a two-step procedure. Alternatively, coupling reagents can be used in a single-step reaction with good yields, which seems to be suitable for organic chemistry laboratory classes. This work was designed to synthesize "N"-hexylcinnamamide through a one-step…

Electrocatalytic hydrogenation of acetol (IUPAC: 1-hydroxy-2-propanone), a species formed upon thermal liquefaction of biomass, can be achieved using inexpensive objects: filter paper, coins, batteries, salts, and water. This simple example demonstrates that "green" chemical transformations can be achieved with familiar items and helps…

In this article, we examine the rotation angle dependence of a hand-made fan-type variable capacitor for use in physics experiments in university classes. We made two circular bakelite plates, and the two terminal plates of the capacitor were 90° fan-type copper disks. The capacitance varied linearly with the rotation angle. The standard deviation…

Due to a growing awareness of environmental issues, green chemistry concepts are increasingly being incorporated into the undergraduate organic chemistry lecture and laboratory component. This minireview summarizes environmentally friendly organic chemistry experiments suitable for undergraduate laboratories. Whenever feasible, LD[subscript 50]…

The bromination of six isomeric alcohols is adapted to a discovery-based organic chemistry laboratory experiment, whereby students are provided an alcohol starting material and are charged with determining the product or product mixture produced using relevant spectroscopic data. The experiment solidifies NMR analysis skills while reinforcing the…

We have developed a new foundation-level course at our institution that links the concept of chemical equilibria from four of the traditional subdisciplines (analytical, biochemistry, inorganic, and physical). The course, entitled Solution and Solid State Chemistry (CHEM 210), is designed to serve our chemistry and biochemistry majors, as well as…

This laboratory experiment introduces upper-division undergraduate analytical chemistry students to liquid chromatography-tandem mass spectrometry (LC-MS/MS) in a forensic application: the analysis of cocaine and metabolites of cocaine in simulated serum ostensibly from drug overdose victims. For this investigation, students developed the…

This three-part laboratory experiment investigates key aspects of the Buchwald-Hartwig amination cross-coupling reaction through guided-inquiry learning strategies. The first part of this experiment utilizes high-throughput experimentation techniques to reinforce, explore, and extend fundamental concepts that are represented in the classroom,…

A practical experiment is described to estimate the distance to a star using simple equipment, suitable for secondary or undergraduate students. The brightness of the star is visually matched to a miniature filament lamp, and its distance inferred from the inverse square law. Students gain an appreciation of astronomical units and practice in…

Infrared (IR) spectroscopy is a vibrational spectroscopic technique useful in chemical, pharmaceutical, and forensic sciences. It is essential to identify chemicals for reasons spanning from scientific research and academic practices to quality control in companies. However, in some university degrees, graduate students do not get the proficiency…

Due to social distancing constraints during the COVID-19 pandemic, several experiments were designed in the Fall 2020 and Spring 2021 semesters in our Electrochemistry and Corrosion elective course to demonstrate electrochemical phenomena and applications at the students' homes with a kit sent by the school. We report here a student-designed…

A comprehensive undergraduate experiment about extraction, separation, and identification of essential oils (EOs) from a natural plant is described. "Acori tatarinowii" Rhizoma (ATR) was used as the raw plant material. Two devices (Soxhlet and Clevenger) with different extraction principles were employed for EO extraction from ATR,…

This paper reports a demonstration of a 90 min on-demand class where a chemical experiment is performed to educate nonscience majors on surfactants. First-year undergraduate students perform the water ball in a water bottle experiment at home and learn about the structure and properties of organic compounds in the demonstration. The experiment is…

This is an easy and cheap experiment where chemistry Masters students can evaluate the role of some metal ions (i.e., Cu[superscript II] and Mn[superscript II]) in dopamine oxidation, related to Parkinsonism. The required prior knowledge is being familiar with the basis of UV-vis spectroscopy. Details of the activity, including procedure and…