Preparative chromatography is one of the most common and important purification techniques in organic chemistry and is employed in laboratories across the globe. In order to facilitate student proficiency with the method, a unique approach for the separation of estragole, ethyl cinnamate, and cinnamyl alcohol using microscale preparative flash…

During COVID-19 remote instruction, instructors were tasked with providing students with authentic laboratory experiences in an out-of-classroom environment. One solution developed for our introductory general chemistry laboratory involved students critiquing readily available technique videos to distinguish between correct and incorrect…

A laboratory experiment was designed to introduce the practical application of biocatalysis in Bachelor and Master courses in biotechnology and medicinal chemistry, respectively. To this aim, the lipase from "Candida rugosa" was characterized (protein concentration and activity), immobilized on a carrier (by hydrophobic adsorption), and…

This paper outlines a comprehensive teaching laboratory course program that centers on titration analysis, a timeless and essential technique in analytical chemistry spanning various disciplines, such as environmental science, medicine, and industry. In these fields, titration analysis is paramount for determining the concentrations of substances…

Despite the growing importance of nanomaterials in numerous industries, most undergraduate chemistry students are unlikely to encounter characterization techniques common in the field during their education. Scanning electron microscopy (SEM) is a common technique for materials characterization widely used in careers chemistry students are likely…

A variety of strategies have been introduced to tackle the issue of laboratory safety in academic settings. These strategies include innovative educational tools as students transition from the classroom into the laboratory, the introduction of policies designed to protect the researchers in the laboratory environment, and the creation of teams of…

The 21st century technology has advanced to become an accessible beacon of education. The physical boundaries of the chemistry laboratory have expanded with the use of innovative virtual lab simulations despite disparate results from previous investigations of student performance comparing virtual lab simulations with traditional laboratory…

Laboratory work has been a common element of science courses at university level for around two centuries, but its practice has been criticised by scholars in the field and related stakeholders. Mainly on a rationale of financial justification and educational efficacy, more evidence for learning has been called for. The aims of this systematic…

Over a decade has passed since faculty members' goals for the undergraduate chemistry instructional laboratory were first investigated on a large, national scale in the United States. This study revisits these goals, using data from a 2022 national survey of chemistry faculty members in the United States (n = 521) to investigate current…

Trace metals when present in crude oil or fuels are of economic significance in refining and to the combustion engines that use them. Herein, we develop a laboratory activity that trains students on how to analyze crude oil samples for ash and trace metal content while giving them the opportunity to acquire skills needed as a quality control…

Photo-oxidation is one of the main causes of oxidative deterioration in food. Understanding of the mechanisms of photo-oxidation is essential for food science students when pursuing careers in food safety and quality assurance. However, few food chemistry laboratories emphasize photo-oxidation. Thus, we develop a laboratory activity that trains…

General chemistry laboratories are a core requirement for nearly all STEM (Science, Technology, Engineering, and Mathematics) majors and have the greatest breadth in disciplines and audience of any STEM course at a university. A bioremediation Course-based Undergraduate Research Experience (CURE) for first-year undergraduate students was developed…

A key part of the practice of chemistry is the analysis of chemical composition, including through gravimetric analysis and spectrophotometry. However, the complexity of doing multiple calculations to obtain analytical evidence, such as that required to determine an empirical formula, presents a challenge if such analytical methods are to be…

In case-based learning, students develop and apply course knowledge to solve tangible and "real life" problems. This practice can enhance student motivation and engagement in the analytical laboratory. In this application of case-based learning students analyze commercially available oils for CBD content. In the state of Texas anyone can…

We present the development and evaluation of "da Vinci's Curse", a chemistry escape room experience designed to consolidate laboratory skills in a fun and interactive setting. Inspired by the maestro, Leonardo da Vinci, the escape room challenges students to complete a series of puzzles in teams to escape "da Vinci's Curse".…