Recently, smart sensing/actuation paper has attracted significant interest due to its potential usage as a sustainable component in future electronics, robotics, and intelligent sensing devices. In acknowledging the importance of this topic for the engagement of students at the university level in conjunction with Industrial Revolution 4.0, it is…

Cyclic voltammetry (CV) is the most popular electrochemical technique for the study of electrode processes. One of the reasons for its popularity is its adjustable timescale which can vary several orders of magnitude simply by varying the rate at which the potential is scanned. Changing the scan rate affects CV features including the current,…

Many types of batteries power an ever-growing number of devices. Electrochemical devices like batteries and fuel cells can, in principle, exceed Carnot efficiency for energy conversion. In this novel laboratory experiment, students explore the partitioning of the enthalpy change of a battery's electrochemical reaction between useful electrical…

An undergraduate electrical conductivity measurement experiment in a physical chemistry lab and basic fitting procedures are presented that allow a characterization of micellar system of hexadecyltrimethylammonium bromide (cetyltrimethylammonium bromide, CTAB) in binary mixture of water and acetonitrile (ACN) as a cosolvent (10%, v/v) at 30.0 °C.…

A "one-pot" method for acquiring kinetic data for the reactions of a series of substituted aromatic esters with potassium hydroxide using [supserscript 13]C NMR spectroscopy is described, which provides an efficient way to obtain sufficient data to demonstrate the Hammett equation in undergraduate laboratories. The method is…

This study proposes a home-assembled, low-cost blue light-emitting diode (LED) photometer that uses simple and low-cost hardware and software, costing about US $150. This 425-nm wavelength photometer is controlled by an 89C51 microcontroller chip. Glucose concentration detection experiments involving enzyme coupling reactions were carried out to…

The use of the Beer-Lambert law in spectroscopy is the core of standard methods for determining a chromophore concentration in a solution. Its application requires an understanding about interaction of light with a colored solution and the use of light emission and light detection devices. We build here a simple electronic circuit formed of…

The teaching of instrumental analysis for many small colleges and high schools continues to be stymied by high-cost, complicated maintenance, high power requirements, and often the sheer bulk of the instrumentation. Such issues have led us to develop inexpensive instruments as part of a SMILE initiative (small, mobile instruments for laboratory…

A laboratory experiment is described in which students fabricate disk-shaped gold and platinum microelectrodes with diameters of 10-50 [mu]m by sealing sodalime glass with metal microwires. The electrodes are characterized by performing cyclic voltammetry in aqueous and acetonitrile solution. Commercial microelectrodes are expensive (cost depends…

An experimental study of ceramic superconductors namely YBa2Cu3O(sub 7-x), which illustrates the use of spectrophotometry, based on the electronic spectra of complexes of Fe(II), Fe(III) and Cu(II) to better understand the stoichiometry of YBCO is described. The results from this experiment are in good agreement with those obtained by the…

A circuit board analysis of the atomic absorption spectroscopy, which is used to measure lead content in a course for nonscience majors, is being presented. The experiment can also be used to explain the potential environmental hazards of unsafe disposal of various used electronic equipments.

Describes laboratory experiments suitable for teaching the principles of digital electronics and computer interfacing to undergraduate chemistry students. Also describes the program for teaching laboratory uses of computers. The program functions to teach principles of computer interfacing while displacing as little chemistry as possible from the…

Provides a reading list for A- and S-level biology. Contains several experiments and demonstrations with topics on: the intestine, bullock corneal cells, valences, the science of tea, automated hydrolysis, electronics characteristics, bromine diffusion, enthalpy of vaporization determination, thermometers, pendulums, hovercraft, Bernoulli fluid…