In the current study, the audiotapes from three hostage-taking situations were analyzed. Hostage negotiator requests to the hostage taker were characterized as either high or low probability. The results suggested that hostage-taker compliance to a hostage negotiator's low-probability request was more likely when a series of complied-with high-probability requests preceded the low-probability request. However, two of the three hostage-taking situations ended violently; therefore, the implications of the high-probability request sequence for hostage-taking situations should be assessed in future research. (Contains 1 figure.)