A microscale isotopic labeling experiment is described for the introductory organic chemistry laboratory course wherein half of the students use sodium borohydride (NaBH[subscript 4]) and the other half use sodium borodeuteride (NaBD[subscript 4]) to reduce acetophenone to 1-phenylethanol and then compare spectral data. The cost is reasonable, and…

Quantitative [superscript 13]C NMR provides a straightforward method of analyzing edible oils in undergraduate chemistry laboratories. [superscript 13]C spectra are relatively easy to understand, and are much simpler to analyze and workup than corresponding [superscript 1]H spectra. Average chain length, degree of saturation, and average…

The double-wall paper cup is an everyday object that can be used in the laboratory to study heat transfer. The experiment described here has been done by physics students aged 12-13 years; it can also be used in a different context to prompt debate about environmental issues.

Natural products are ubiquitous in nature but do not form a large proportion of the A-level syllabuses in the UK. In this article we briefly discuss a small selection of natural products, focusing on alcohols, aldehydes and ketones, and alkaloids. We then outline two natural product experiments that are suitable for A-level chemistry clubs or…

Generating enthusiasm among nonscience majors in a laboratory course is a difficult task. Often, students are asked to perform a precipitation reaction, only to collect and then safely dispose of the solid without detailing composition, properties, or uses. In an effort to keep the students engaged, this laboratory exercise presents an innovative…

Enzyme purification, characterization, and identification are some of the best ways to introduce undergraduate students to many aspects of biochemistry, particularly as part of project-based learning (PBL). These kinds of multi-step laboratory experiments not only help students to better understand basic biochemistry concepts but also serve to…

To improve the teaching and learning materials for a curriculum it is important to incorporate the findings from educational research. In light of this, we present creative exercises and experiments to elicit, confront and resolve misconceptions in geometrical optics. Since ray diagrams can be both the cause and the solution for many…

Students come to class with little understanding about torque, angular velocity, and angular acceleration despite the fact that these physical science concepts are frequently observed. For example, torque occurs when car and bicycle tires rotate, the movement of fishing pole when hooking a fish, and when a person uses a hammer to drive in a nail.…

Electrochemistry is primarily taught in first-year undergraduate courses through batteries; this lab focuses instead on corrosion to apply electrochemical concepts of electrolytes, standard reduction potentials, galvanic cells, and other chemistry concepts including Le Chatelier's Principle and Henry's Law. Students investigate galvanic corrosion…

This paper presents a system for remote monitoring of turbidity data that can detect light intensity and temperature using a microcontroller and the Internet of Things. The system comprises a light dependent resistor and infrared temperature sensor interfaced with an ESP-12E microcontroller, a programmable data acquisition platform; together these…

The purpose of this paper is to present and discuss an alternative solution to an experimental problem given to high school students in the XXII Ibero-American Physics Olympiad held by Colombia this year. From the measurements of electric current and potential difference across a small tungsten filament lamp students should find the dimensions of…

This experiment prepares a large (M[subscript r]: 1821 g mol[superscript -1]) triple helicate complex quickly in one pot from inexpensive starting materials. The protocol illustrates the power of self-assembly in a simple manner that is suitable for second-year general chemistry students using reversible imine bond and metal-ligand bond formation.…

Laboratory reports written in the style of a standard scientific article are commonly used to assess student learning in biochemistry laboratory courses. While most students can complete the Materials and Methods or Results sections successfully, many have difficulty with the Introduction and Discussion. They fail to place their data in a larger…

An undergraduate experiment for the organic laboratory is described that utilizes microwave heating to prepare 5- substituted 1H-tetrazole derivatives through a (3 + 2) cycloaddition between aryl nitriles and sodium azide. The reaction mixture is analyzed by thin layer chromatography. The products are purified through an acid-base extraction and…

This paper describes an undergraduate laboratory experiment where students study the heating behavior of magnetic nanoparticles in the presence of alternating magnetic fields. Average score on the post-test was 45±12% for students who completed the lab online, versus 43±11% for those doing the activity hands-on. Post-test scores were significantly…