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Self-Assembly, Guest Capture, and NMR Spectroscopy of a Metal-Organic Cage in Water
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Go, Eun Bin; Srisuknimit, Veerasak; Cheng, Stephanie L.; Vosburg, David A. – Journal of Chemical Education, 2016
A green organic-inorganic laboratory experiment has been developed in which students prepare a self-assembling iron cage in D[subscript 2]O at room temperature. The tetrahedral cage captures a small, neutral molecule such as cyclohexane or tetrahydrofuran. [Superscript 1]H NMR analysis distinguishes captured and free guests through diagnostic…
Descriptors: Science Instruction, Science Laboratories, Laboratory Experiments, Science Experiments